Wrap-up
91%
Writing the spec — what goes on the print
An annotated nitriding callout template a competent vendor can hit and an incompetent one will refuse, with the eight elements that turn a wish into a spec.
Tying it together
Common spec mistakes that doom the job
Calling out HRC alone with no scale and no load. The Rockwell C reading on a thin case is meaningless; the vendor can deliver an HRC number that translates to a case that fails in service.
"Case depth 0.020 inch" with no definition. Total NHD and effective case depth can differ by 2× on the same part. The vendor picks the favorable definition.
"Minimize white layer" without a number. A vendor running a high-Kn cycle will produce 15 µm of compound layer and document that they "minimized" relative to what they could have grown.
Quoting AMS 2759/10 without specifying class. The standard has classes with different Kn ranges, different case depth requirements, and different certification levels. AMS 2759/10B Class 1, Class 2, and Class 3 are different specifications.
No substrate condition on the print. The vendor either asks (delay) or guesses (failure). H13 at 50 HRC and H13 in the annealed state nitride differently, and the vendor cannot tell from looking at the part.
Up next: vendor selection.
Sources
- SAE International, AMS 2759/10B: Automated Gaseous Nitriding Controlled by Nitriding Potential. https://www.sae.org/standards/content/ams2759/10b/
- SAE International, AMS 2759/12: Gaseous Nitrocarburizing, Automatically Controlled by Potentials. https://www.sae.org/standards/content/ams2759/12/
- ISO, ISO 18203:2016 — Steel — Determination of the thickness of surface-hardened layers. https://www.iso.org/standard/61748.html
- GWP Materialtechnologie, Nitriding hardness depth (NHT) according to DIN 50190-3. https://gwp.eu/en/leistung/nitriding-hardness-depth-nht-according-to-din-50190-3/
- ASTM International, ASTM E384 — Standard Test Method for Microindentation Hardness of Materials. https://www.astm.org/news/microindentation-hardness-mj10
- Advanced Heat Treat Corp, Evaluating Case Depth for Case Hardening Treatments. https://www.ahtcorp.com/articles/blog/evaluating-case-depth-for-case-hardening-treatments/
- Pye, D. Practical Nitriding and Ferritic Nitrocarburizing, ASM International, 2003. https://dl.asminternational.org/technical-books/monograph/172/Practical-Nitriding-and-Ferritic-Nitrocarburizing